✦ LIBER ✦

A two-step synthesis of pyridoxatin analogues

✍ Scribed by Barry B. Snider; Lu Qing

Book ID: 104215597
Publisher: Elsevier Science
Year: 1994
Tongue: French
Weight: 388 KB
Volume: 35
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(00)75830-8

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✦ Synopsis

Abstcactz condensation of 4-hydroxy-2-p@onc (4) with citnmellal (10) affords oquinone methii intermediate 11, whichlieactsfurthertogiveinvem ebxtronDi&-Aldcradducal2(46%)and 16(25%)a1~lencadduct14(28%).

Oxidathn of 12 and 14 by Sammcs' pmccdum aft&s pyriUoxatia analogties 13 (54%) and IS (48%).

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