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A two-step synthesis of diaminofurazan and synthesis of N-monoarylmethyl and N,N′-diarylmethyl derivatives

✍ Scribed by Alexander K. Zelenin; Mark L. Trudell

Publisher
Journal of Heterocyclic Chemistry
Year
1997
Tongue
English
Weight
277 KB
Volume
34
Category
Article
ISSN
0022-152X

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✦ Synopsis

Abstract

Diaminofurazan (1) was synthesized from glyoxal (2) by an improved two‐step procedure. The N‐mono‐arylmethyl derivatives 4a‐e and N‐N'‐diarylmethyl derivatives 5a‐e of 1 were prepared in good yields by reductive alkylation with the corresponding aryl aldehydes.

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