Carbon-13 CPMAS spectra have been recorded for anhydrous and monohydrate forms of androstanolone. The results are discussed in relation to crystallography. The anhydrous form gives crystallographic splittings in the spectra arising from non-equivalent molecules in the unit cell. The spectra are assi
A Theory for Cross-Polarization NMR of Nonspinning and Spinning Samples
โ Scribed by David Marks; Shimon Vega
- Publisher
- Elsevier Science
- Year
- 1996
- Tongue
- English
- Weight
- 336 KB
- Volume
- 118
- Category
- Article
- ISSN
- 1064-1858
No coin nor oath required. For personal study only.
๐ SIMILAR VOLUMES
## Abstract The 13C chemical shifts of the CP/MAS NMR for ferrocene derivatives have been measured. Copyright ยฉ 2002 John Wiley & Sons, Ltd.
Zero-order average-Hamiltonian theory is used to extend the product-operator description of coherent spin-spin cross-polarization to the case of a spin-12 coupled to a general object, like a molecular rotor or a quantum oscillator. The object, which is not necessarily in a Boltzmann equilibrium stat
The cross-polarization dynamics between 1 H and 19 F in a Viton-type fluoroelastomer were studied using 19 F magic angle spinning (MAS) and 1 H ! 19 F cross-polarization (CP)/MAS NMR at 188.29 MHz. The phenomenological theory of spin thermodynamics based on the spin temperature hypothesis was employ