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A Tetranuclear Niobium Oxo Acetate Complex. Synthesis, X-ray Crystal Structure, and Characterization by Solid-State and Liquid-State NMR Spectroscopy

✍ Scribed by Steunou, Nathalie; Bonhomme, Christian; Sanchez, Clément; Vaissermann, Jacqueline; Hubert-Pfalzgraf, Liliane G.


Book ID
126924303
Publisher
American Chemical Society
Year
1998
Tongue
English
Weight
330 KB
Volume
37
Category
Article
ISSN
0020-1669

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A simple molecule with a complex crystal
✍ Klaus Eichele; Christiane Nachtigal; Susanne Jung; Hermann A. Mayer; Ekkehard Li 📂 Article 📅 2004 🏛 John Wiley and Sons 🌐 English ⚖ 174 KB

## Abstract A comprehensive ^31^P solid‐state NMR study of Ru(η^1^‐Ph~2~PCH~2~CH~2~OCH~3~)~2~(η^2^‐en)Cl~2~ (en = ethylenediamine) (1), by 1D (contact time variation, inversion–recovery, SPARTAN) and 2D techniques (homonuclear __J__‐resolved, SECSY) indicated that the crystal structure of 1 should