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A synthetic route to 1,2,4,5-tetrahydro-3H-benz[e]indoles

✍ Scribed by S.L. Keely Jr; A.J. Martinez; F.C. Tahk

Publisher
Elsevier Science
Year
1969
Tongue
French
Weight
198 KB
Volume
10
Category
Article
ISSN
0040-4039

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✦ Synopsis

We describe here the synthesis In two steps from the appropriately substituted t3-tetralones of 3-methyl-1,2,4,5-tetrahydro-8H-benz[e]indole, la, and of its 8,9-dimethoxy analog, lb. Insofar as we are aware, no compounds

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In the title compound, C 19 H 15 BrN 2 O 4 S, the orientations of the phenylsulfonyl and 2-bromo-4,5-dimethoxybenzyl substituents with respect to the indole moiety are influenced by intramolecular C-HÁ Á ÁO and C-HÁ Á ÁBr interactions. The sulfonyl-bound phenyl ring forms a dihedral angle of 86.9 (1

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