## Abstract Labeled silver carbonate was prepared from barium carbonateβ^13^C or β^14^C and aqueous silver nitrate in 95 to 100% yield. Diethyl carbonateβ^13^C or β^14^C was generated in 60 to 85% overall yield by treatment of labeled silver carbonate with ethyl iodide and tetraethylammonium iodide
A Synthesis of 1-C 14 -Labeled Diethyl Ether
β Scribed by Burtle, Jerome G.; Turek, William N.
- Book ID
- 126136806
- Publisher
- American Chemical Society
- Year
- 1954
- Tongue
- English
- Weight
- 135 KB
- Volume
- 76
- Category
- Article
- ISSN
- 0002-7863
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π SIMILAR VOLUMES
Isobutyl [3-14C] cyanoacrylate and diethyl [3-14C] methylidenemalonate were synthesized by the intermediate of their protective Diels-Alder adduct with anthracene. These adducts (&&,I were obtained in a one-pot procedure by Knoevenagel condensation of p4C] paraformaldehyde with isobutyl cyanoacetate
A method is described for the preparation of 1,2-dialkyl glycerol ethers starting from 3-tetrahydropyranyl-glycerol and alkyl methanesulfonates. By reaction of an excess of 1,2-dialkyl glycerol ethers and (l-14C)-alkyl methanesulfonares 14C-labelled trialkyl glycerol ethers are obtained in good yie