𝔖 Bobbio Scriptorium
✦   LIBER   ✦

A study of the reversibility of friedel-crafts C-acetylations by means of 14C-labelling

✍ Scribed by M. Frangopol; A. Genunche; N. Negoita; P.T. Frangopol; A.T. Balaban

Publisher
Elsevier Science
Year
1967
Tongue
French
Weight
268 KB
Volume
23
Category
Article
ISSN
0040-4020

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

Synthesis of a 11C-labelled taxane deriv
Synthesis of a 11C-labelled taxane derivative by [1-11C]acetylation
✍ P. Mäding; J. Zessin; U. Pleiß; F. Füchtner; F. Wüst 📂 Article 📅 2006 🏛 John Wiley and Sons 🌐 French ⚖ 173 KB

## Abstract The ^11^C‐labelling of the taxane derivative BAY 59‐8862 (**1**), a potent anticancer drug, was carried out as a module‐assisted automated multi‐step synthesis procedure. The radiotracer **[^11^C]1** was synthesized by reacting [1‐^11^C]acetyl chloride (**6**) with the lithium salt of t

Preparation of bromo[1-14C]acetyl-coenzy
Preparation of bromo[1-14C]acetyl-coenzyme A as an affinity label for acetyl-coenzyme A binding sites
✍ Denise M. Lowe; Philip K. Tubbs 📂 Article 📅 1983 🏛 Elsevier Science 🌐 English ⚖ 769 KB

Bromo[1-14C]acetyl-CoA has been prepared from CoASH and the N-hydroxysuccinimide ester of bromo[1-14C]acetic acid, and unlabeled bromoacetyl-CoA by reaction of CoASH with bromoacetyl bromide. The products were purified by high-pressure liquid chromatography. Purified bromoacetyl-CoA was characterize

Rapid synthesis of 14C forskolin by a ro
Rapid synthesis of 14C forskolin by a route suitable for 11C labeling
✍ T. Sasaki; I Ogihara-Umeda; H. Nishigori; S. Ikegami; M. Senda; K. Kitani; K. Og 📂 Article 📅 1991 🏛 John Wiley and Sons 🌐 French ⚖ 400 KB

## Abstract Radiolabeled forskolin was synthesized by acetylation of deacetylforskolin with ^14^C‐labeled acetic acid in the presence of dicyclohexylcarbodiimide. Separation of labeled forskolin of greater than 97% radiochemical purity was achieved by HPLC with a reversed‐phase column. The synthesi