A simple two-step method for the conversion of [3H]cortisol to [3H]-11-ketotestosterone
β Scribed by P.Mark Lokman; L. Irwin; Leonard F. Blackwell; Peter S. Davie; Mervyn Thomas; Graham Young
- Book ID
- 117213869
- Publisher
- Elsevier Science
- Year
- 1997
- Tongue
- English
- Weight
- 428 KB
- Volume
- 62
- Category
- Article
- ISSN
- 0039-128X
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π SIMILAR VOLUMES
The combination of P 4 S 10 , sulfur, and hexamethyldisiloxane converts 3-oxoesters to 3H-1,2-dithiole-3thiones in yields generally superior to those obtained with Lawesson's reagent and without the need for chromatography to remove large amounts of phosphorous-containing byproducts.
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