In flow-injection analysis (FJA) systems with electroosmotic flow (EOF), the maximum permissible sample throughput is a function of the electric field strength, capillary length and injection volume. The relation behveen the various parameters is theoretically and experimentally discussed. Experimen
A simple multifunctional valve for flow injection analysis
✍ Scribed by S. Storgaard Jørgensen; Katrine Maria Petersen; Lone Anette Hansen
- Publisher
- Elsevier Science
- Year
- 1985
- Tongue
- English
- Weight
- 451 KB
- Volume
- 169
- Category
- Article
- ISSN
- 0003-2670
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✦ Synopsis
A simple and versatile pneumatically-operated two-layer rotary valve is described for simultaneous introduction of samples and diversion of analytical streams in flow injection analysis. Examples of applications include valve configurations with time-controlled sample volume and with loop-controlled sample volumes in one or two loops; both configurations are useful in routine analyses of samples of highly varying analyte concentrations. The usefulness of the valve for ion-exchange preconcentration procedures is also demonstrated.
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A micromethod for ochratoxin A detection in human sera by flow injection technique is described. The method requires 50 pl of sera, and it is designed to distinguish samples containing less than 10 ng ochratoxin A per ml. The method is based on fluorescence measurement following a simple extraction
An injection valve with a small internal loop actuated by pneumatic switching was used for high-speed gas chromatography (GC). Small internal diameter (50 and 100 p m i.d.1 open tubular columns were used for investigations of the injector performance. Several valve injection systems have been tested