A simple method for separating polar steroids from the liquid scintillation phosphor

✍ Scribed by Richard S. Rivlin; Hildegard Wilson

• Publisher: Elsevier Science
• Year: 1963
• Tongue: English
• Weight: 149 KB
• Volume: 5
• Category: Article
• ISSN: 0003-2697
• DOI: 10.1016/0003-2697(63)90127-1

✦ Synopsis

intermediates of fatty acid metabolism were checked and the Rf values obtained with the solvent mixture described are given in Table 1. The TABLE 1 R, VALUES OF ilcy~ HYDROXAMATES AND METHYL ISOXAZOLONE IN METHYLENE CHLORIDE:~~UTANOL:~CETIC ACIDZNATER Compound __-Hydroxamates: Malonyl monop-Hydroxybutyryl-Acetyl-&Hydroxy+methylglutaryl mono-Butryryl-Hexanoyl-Methyl isoxazoione RI 0.0 0.23 f 0.02 0.35 f 0.02 0.68 F 0.02 0.75 + 0.02 0.90 Y!r 0.02 0.50 5 0.03 table includes the Rf of methyl isoxazolone, the reaction product of acetoacetyl CoA and hydroxylamine (3).