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A simple, inexpensive synthesis of dipotassium cyclooctatetraenide, K2C8H8

✍ Scribed by Evans, William J.; Wink, Donald J.; Wayda, Andrea L.; Little, David A.

Book ID
126861459
Publisher
American Chemical Society
Year
1981
Tongue
English
Weight
653 KB
Volume
46
Category
Article
ISSN
0022-3263

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A chain-like zincophosphate [Zns(HPO4)8(H2PO4)8]\*[(C2HsN)s] -4H20 was obtained at room temperature from a ZnO/PzOs/dimethylamine/H20 mixture. The crystal structure was determined by single crystal X-ray diffraction. The symmetry is monoclinic a=l,26450(7)nm, b=l.08477(5)nm, c=1.46311(4)nm, 13=98.79