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A ruthenium-catalyzed coupling of alkynes with 1,3-diketones

✍ Scribed by Megan K. Pennington-Boggio; Brian L. Conley; Travis J. Williams

Book ID
116680402
Publisher
Elsevier Science
Year
2012
Tongue
English
Weight
808 KB
Volume
716
Category
Article
ISSN
0022-328X

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1,3-Diketones were reduced to 1,3-diols by using RuCl[N-(tosyl)-1,2-(diphenylethylenediamine) (h 6 -arene)] in the presence of formic acid and triethylamine. 1,3-Diols were obtained in good chemical yields and with high ee when symmetrical diketones were reduced.