## Abstract A modified Andreasen sedimentation method is described for the analysis of the DDT and carrier constituents of DDT dispersible powders. As an illustration of the use of the method, a 1% (w/v) aqueous suspension of the powder is sampled with a pipette at four different times from the co
A rapid method for the determination of the specific surface and mean particle size of black powders
โ Scribed by Frith, F. ;Mott, R. A.
- Publisher
- Wiley (John Wiley & Sons)
- Year
- 1946
- Weight
- 814 KB
- Volume
- 65
- Category
- Article
- ISSN
- 0368-4075
No coin nor oath required. For personal study only.
โฆ Synopsis
mixed acids from the origiunl oil (77 g.) \rere dissolved in light petroleum nt 0" (wlieu 10.0 g. of resin scpsrnted) i t i d subsequeutly stcam-distilled (yielding 0.95 g. volatile mnterisl, cquir. 156 -1) prior to conversiou into nictliyl esters. Tliese were fairly rendily hydrogennted r r t 100" in presence of Rnney nickel, tile product being again stenm-distilled, and the residual esters (48.3 g., iodiue value 14.0) frnctionated iu it ~*iicuum. Again, n rcsitluc (6.8 g.) of utidistilled esters remined (cquir. 371 -5, iodiric rnluc 71), cvideiltly representing " resinous " coinpound which hnd not bee^ coiupletely removed in the eirrlier sepurntion from light ~ictrolcuni. The frnctionntioii dntn in tlik crperin~cnt sl~o~~vctl t l ~c presence of 1.1 . I % pnluutic acid i l l thc mixed liydrogennted ncids ; this corrcspotids to 11 .Syo palmitic acid in the original niisture of ncitls ill wliioh :ill the resiuous derivative w i s still present, : i d thus nccortls sntiufnctorily with tlie preceding dcterniinirtioii.
Roughly spenking, T. occidcri(uli.7 seed Lit contaius &out equnl proportions of a-eltrcosteiiric, liiioleic, oleic, sntuntrd, nnd the resinous or uon-fntty :icid, pilinitic acid forming about two-thirds of the snturnted ticids. It tliercfore sceins to linre no obvious technical prospects, but is interestiug from the more ncndeinic standpoint in its glyceride content of n non-Lit$ ncid of pcculinr constitutiotl, and in the nuirked differelice I,etireen its conipoueut ncids uud thosc of the niore convcntioual seed fat of the reltrtcd species 2'. p d a t a , the component zrcids of which :ire pdmitic 33, stcaric 14, olcic 14, linolcic 36, liuolciiic 3% (wt.). Noreover, only oue other seed fat17 of the Cucurbitncene lins I)ecii reported to coutniu uiisaturnted ncid.9 other tlinn those of tho iion-conjugated fatty Clg series.
๐ SIMILAR VOLUMES
A sinipliliid forin Inns l~ecii duvulolrctl of tho nir-prnienbility nppnrntus described by I.cn and Nurse for rucnsiirin tho rpccific surfiico of ponders. Crown copyright rcsorc\*ed.
A method i s described f o r the topological localization of c e l l surface anionic s i t e s using positively charged colloidal iron hydroxide (Gasic e t a l . , Lab. Invest. 18, 63 [1968]). Purified glutaraldehydc-fixed plasma c e l l membranes o r glutaraldehyde-fixed lysed c e l l s a r e mount