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A Practical Approach to Synthesize the C(9) –C(24) Fragment of (+)-Discodermolide

✍ Scribed by Zengsheng Yin; Xuyi Yue; Xiangjun Deng; Fengling Qing

Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
273 KB
Volume
28
Category
Article
ISSN
0256-7660

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Toward a Total Synthesis of Pristinamycin II B ; a Chiron Approach to a C-9/C-16 Fragment. -Starting from readily available (S)-malic acid derivative (I), an appreciable amount (ca. 2 g) of the title fragment (XV) is prepared using the Grignard reaction of the propargyl diol (VI) as the key step. T