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A Novel trans-1,2-Dimethyldiaziridine–Silver Nitrate Complex: Synthesis and Molecular and Crystal Structure

✍ Scribed by Gennadii V. Shustov; Alexander B. Zolotoi; Sergei V. Konovalikhin; Lev O. Atovmyan; Remir G. Kostyanovsky

Book ID
111729754
Publisher
Royal Society of Chemistry
Year
1995
Tongue
English
Weight
114 KB
Volume
5
Category
Article
ISSN
0959-9436

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The reaction of 4-amino-6-methyl-1,2,4-triazine-3(2 H)-thione-5-one (AMTTO) with silver(I) nitrate in methanol gives the complex [Ag(AMTTO) 2 ]NO 3 (1). 1 was characterized by IR and 13 C NMR spectroscopy and by an X-ray structure analysis [space group C2/c, Z = 4, lattice dimensions at ±80 °C: a =