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A novel synthetic approach to 4-acetamido-1-arylindazoles via Semmler–Wolff rearrangement of 1-aryl-6,7-dihydro-5H-indazol-4-one oxime

✍ Scribed by Manjunatha, Sulur G.; Bachu, Sreekanth; Kadambar, Vasantha Krishna; Murugan, Andiappan; Ramasubramanian, Sridharan; Ramachandra, Puranik; Nambiar, Sudhir

Book ID
121759966
Publisher
Elsevier Science
Year
2014
Tongue
French
Weight
244 KB
Volume
55
Category
Article
ISSN
0040-4039

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A simple and efficient synthesis of 2-(cyclohexylamino)-6,7-dihydro-3-aryl-1H-indole-4(5H)-ones was achieved via a one-pot multi-component reaction of cyclohexyl isocyanide, an aldehyde, a 1,3-dicarbonyl compound, and ammonium acetate in the presence of a catalytic amount of KHSO 4 in acetonitrile.