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A novel synthesis of 1,4-dihydrobenzo[c]-1,5-naphthyridin-2(3H)-ones from pyrrolo[1,2-b]isoquinolines

✍ Scribed by Martin, Lawrence L.; Scott, Susan J.; Agnew, Marc N.; Setescak, Linda L.

Book ID: 123621064
Publisher: American Chemical Society
Year: 1986
Tongue: English
Weight: 599 KB
Volume: 51
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo00369a026

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## Abstract Heating of hexahydro‐5__H__‐pyrrolo[2,1‐__c__][1,4]benzodiazepine‐2,5,11‐trione in boiling phosphoryl chloride led to a rearranged product like 3,5‐dichlorobenzo[__h__][1,6]naphthyridine. This structure was established from X‐ray diffraction analysis.