A Novel Recyclable Sulfur Monoxide Transfer Reagent
โ Scribed by Grainger, Richard S.; Procopio, Alberto; Steed, Jonathan W.
- Book ID
- 126160340
- Publisher
- American Chemical Society
- Year
- 2001
- Tongue
- English
- Weight
- 59 KB
- Volume
- 3
- Category
- Article
- ISSN
- 1523-7060
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๐ SIMILAR VOLUMES
## Abstract Various diacyl sulfides were synthesized by reaction of acyl chlorides with LiAlHSH. Reaction of glutaryl chloride with LiAlHSH afforded glutaric thioanhydride. ยฉ 2003 Wiley Periodicals, Inc. Heteroatom Chem 14:633โ635, 2003; Published online in Wiley InterScience (www.interscience.wile
A commercially available and inexpensive compound, 3-amino-1,2,4-dithiazole-5-thione (ADTT), has been attached onto a hydroxyl resin via a succinic acid linker. The polymer-supported ADTT is an efficient sulfur-transfer reagent for the solution-phase synthesis of phosphorothioates.