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A NMR shift method for determination of the enantiomeric composition of hydroperoxides formed by lipoxygenase

✍ Scribed by Cornelis P.A. Van Os; Maarten Vente; Johannes F.G. Vliegenthart

Book ID
115737761
Publisher
Elsevier Science
Year
1979
Tongue
English
Weight
545 KB
Volume
574
Category
Article
ISSN
0005-2760

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Determination of the enantiomeric purity
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✍ J. Belleney; C. Bui; F. J. Carriere πŸ“‚ Article πŸ“… 1990 πŸ› John Wiley and Sons 🌐 English βš– 481 KB

## Abstract The enantiomeric purities of disubstituted β‐lactams were determined by ^1^H and ^13^C NMR spectroscopy using tris[3‐(trifluoromethylhydroxymethylene)‐d‐camphorato]europium(III), Eu(tfc)~3~, as a chiral shift reagent. Using a [Eu(tfc)~3~]/[lactam] ratio of 0.5, most of the resonances we