A New Type of Hexanuclear Iron(III) Hydr
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Dr. Charlie J. Harding; Richard K. Henderson; Dr. Anne K. Powell
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Article
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1993
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John Wiley and Sons
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English
⚖ 378 KB
To a solution of (S)-1 a (290 mg, 1 mmol) in dry T H F (10 mL) at 0 'C was added dropwise nBuLi (0.7 mL of a 1.6 M solution. 1.1 mmol) under argon. The dark solution was stirred at 0 'C for 15 min and 2 h at room temperature. The mixture was cooled to 0 C and iodomethane (120 pL, 2 mniol) was inject