✦ LIBER ✦

A new route to the synthesis of multi-tritiated methyl iodide

✍ Scribed by Manouchehr Saljoughian; Hiromi Morimoto; Henry Rapoport

Book ID: 103920395
Publisher: Elsevier Science
Year: 1988
Weight: 61 KB
Volume: 39
Category: Article
ISSN: 0883-2889
DOI: 10.1016/0883-2889(88)90382-6

No coin nor oath required. For personal study only.

✦ Synopsis

The purpose o£ this comunication is to report on the various aspects of the tritium labelling of the 2-~4-(3-Chlorophenyll-l-piperazinylO ethanol (CI-Alkanol) to sinthesize arylpropionic esthers (analgesic drugs) labelled in the .~icohol moiety, Prior to labelling, thermic stability of CI-Alkanol was studied. The temperature selected for the heterogeneous catalytic exchange of this alcohol in tritated water was 100°0. A satisfactory labelling of i.~ wasaccomplished within 24 hours and 75% acetic acid; under these conditions the unaffected Ci-Alkanol amounted to 37~.

📜 SIMILAR VOLUMES

A New Route to the Synthesis of Long-Cha

A New Route to the Synthesis of Long-Chain Methyl α-Chlorooxoalkanoates.

✍ Abdul Rauf; Shabana Ahmad 📂 Article 📅 2006 🏛 John Wiley and Sons ⚖ 17 KB

## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 200 leading journals. To access a ChemInform Abstract, please click on HTML or PDF.

A practical laboratory route to the synt

A practical laboratory route to the synthesis of trideuteriomethyl-[13C] iodide

✍ Gregory S. Coumbarides; Jason Eames; Neluka Weerasooriya 📂 Article 📅 2003 🏛 John Wiley and Sons 🌐 French ⚖ 74 KB

## Abstract A practical synthetic laboratory route for the synthesis of trideuteriomethyl‐[^13^C] iodide (^13^CD~3~I) (from tetradeuterio‐[^13^C]‐methanol and hydriodic acid) is described. We comment on the experimental protocol, and the use of water as an ‘additive’ to improve the synthetic yield.

A Succinct Route to the Synthesis of Mul

A Succinct Route to the Synthesis of Multi-Labeled [D, 13C] α-Methyl Aromatic Ketones.

✍ Gregory Socrates Coumbarides; Jason Eames; Neluka Weerasooriya 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 37 KB

A new route to substituted 3-methoxycarb

A new route to substituted 3-methoxycarbonyldihydropyrans; enantioselective synthesis of (?)-methyl elenolate

✍ Hatakeyama, Susumi; Ochi, Noriko; Numata, Hirotoshi; Takano, Seiichi 📂 Article 📅 1988 🏛 The Royal Society of Chemistry 🌐 English ⚖ 236 KB

A new route to the synthesis of coumesta

A new route to the synthesis of coumestans

✍ Darbarwar, Malleshwar ;Sundaramurthy, V. ;Rao, N. V. Subba 📂 Article 📅 1974 🏛 Springer-Verlag 🌐 English ⚖ 186 KB

Crossed molecular beam synthesis of a ne

Crossed molecular beam synthesis of a new compound, methyl fluoride iodide (CH3IF)

✍ Farrar, J. M.; Lee, Y. T. 📂 Article 📅 1974 🏛 American Chemical Society 🌐 English ⚖ 362 KB