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A practical laboratory route to the synthesis of trideuteriomethyl-[13C] iodide

โœ Scribed by Gregory S. Coumbarides; Jason Eames; Neluka Weerasooriya

Publisher
John Wiley and Sons
Year
2003
Tongue
French
Weight
74 KB
Volume
46
Category
Article
ISSN
0022-2135

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โœฆ Synopsis

Abstract

A practical synthetic laboratory route for the synthesis of trideuteriomethylโ€[^13^C] iodide (^13^CD~3~I) (from tetradeuterioโ€[^13^C]โ€methanol and hydriodic acid) is described. We comment on the experimental protocol, and the use of water as an โ€˜additiveโ€™ to improve the synthetic yield. Copyright ยฉ 2003 John Wiley & Sons, Ltd.

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