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A New Route to 3- and 2,6-Substituted Fluorenes 2

โœ Scribed by WEISBURGER, ELIZABETH K.; WEISBURGER, JOHN H.

Book ID
125961483
Publisher
American Chemical Society
Year
1958
Tongue
English
Weight
802 KB
Volume
23
Category
Article
ISSN
0022-3263

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6-Alkyl-and 6-(1-alkenyl)-5-iodo-2-pyrones, which are available as major products by reaction of the corresponding (Z)-2-en-4-ynoic acids with iodine and NaHCO 3 in CH 3 CN, undergo insertion of activated zinc metal into their carbon iodine bond to provide the corresponding 5-(iodozinc)-2-pyrones. H