𝔖 Bobbio Scriptorium
✦   LIBER   ✦

A new refinement of the orthorhombic polymorph of acet­amide

✍ Scribed by Bats, Jan W. ;Haberecht, Monika C. ;Wagner, Matthias

Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
339 KB
Volume
59
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

Crystals of orthorhombic acetamide, C 2 H 5 NO, were obtained from a mixture of ethyl acetate and dilute ammonia. The previously reported structure [Hamilton (1965). Acta Cryst. 18, 866±870] was con®rmed, with two molecules in the asymmetric unit. The molecules are hydrogen bonded to form columns. Neighboring columns are connected by weak intermolecular CÐHÁ Á ÁO interactions.

📜 SIMILAR VOLUMES

An ortho­rhom­bic polymorph of myo-inosi
An ortho­rhom­bic polymorph of myo-inositol
✍ Khan, Uzma ;Qureshi, Rizwana A. ;Saeed, Sadaf ;Bond, Andrew D. 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 116 KB

The title compound, C 6 H 12 O 6 , has been obtained from the ethanol fraction of the aerial part of the plant Incarvillea emodi (Wall. ex Royle) Chatterjee, after recrystallization from ethanol/ethyl acetate (60:40). Each molecule is involved in 12 hydrogen bonds, as has been found in other reporte

The orthorhombic polymorph of pyrazine-2
The orthorhombic polymorph of pyrazine-2-carboxylic acid revisited
✍ Małecki, Jan Grzegorz ;Kruszynski, Rafal ;Kusz, Joachim 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 782 KB

The crystal structure of the orthorhombic polymorph of the title compound, C 5 H 4 N 2 O 2 , was previously reported in the space group Pna2 1 [Takusagawa, Higuchi, Shimada, Tamura & Sasada (1974). Bull. Chem. Soc. Jpn, 47, 1409Jpn, 47, -1413]]. Redetermination of this structure shows that the space

A new monoclinic polymorph of anhydrous
A new monoclinic polymorph of anhydrous zinc acetate
✍ He, Hongshan 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 247 KB

Single-crystal X-ray study T = 293 K Mean (C-C) = 0.005 A R factor = 0.035 wR factor = 0.097 Data-to-parameter ratio = 15.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.