A New Process for the Preparation of Ethers
โ Scribed by TUTTON, A. E.
- Book ID
- 109423853
- Publisher
- Nature Publishing Group
- Year
- 1893
- Tongue
- English
- Weight
- 268 KB
- Volume
- 49
- Category
- Article
- ISSN
- 0028-0836
- DOI
- 10.1038/049184b0
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๐ SIMILAR VOLUMES
We wish to report a new method for the prepamtion of trimethylsilyl (TMS) ethers frcm alcohols under mildly acidic conditions. This compliments the most common procedure for the prepamtion of this popular protecting group which uses TA4.S chloride and a base like triethylamine. ## 2,3 Our approac
## Swnmary: T-butyl 2,2,2-trichloroaceiimi&e (l), reaa?ly prepared by addition of t-butawl to trichloroacetonitrile, is an efficient reagent for the preparation of t-butyl ethers and esters in the presence of a catalytic amount of boron trifhon& etherate. Traditional methods for the preparation of