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A new hydroxylation route: introduction of the trimethylsilyloxy group

✍ Scribed by G.M. Maume; E.C. Horning


Book ID
104239015
Publisher
Elsevier Science
Year
1969
Tongue
French
Weight
174 KB
Volume
10
Category
Article
ISSN
0040-4039

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Solutions of (4j in organic solvents display an intensive blue fluorescence and in aqueous mineral acids a blue-green fluorescence. In the N M R spectrum (CDC13) a singlet occurs at T = 0.87, which is ascribed to the protons H-1 and H-3 (the neighboring protons to the ring nitrogen); the