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A New Catalyst for the Selective Oxidation of Butane and Propane

โœ Scribed by Mark E. Davis; Christopher J. Dillon; Joseph H. Holles; Jay Labinger


Publisher
John Wiley and Sons
Year
2002
Tongue
English
Weight
64 KB
Volume
114
Category
Article
ISSN
0044-8249

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โœ Kenneth D. M. Harris; Dr. Wataru Ueda; Prof. Dr. John M. Thomas; Dr. Gallienus W ๐Ÿ“‚ Article ๐Ÿ“… 1988 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 296 KB

The didehydrooxepane system 4a (326 mg, 1.0 mmol) in anhydrous THF ( 5 mL) was treated under argon with nBuaNF (1.0 M solution in THF, 1.2 mL, 1.2 mmol) at ambient temperature and then stirred at 45ยฐC for 8 h. Removal of the solvent, followed by flash column chromatography (silica, 20% ether in petr