A simple and general standard-addition method for a single-component determination is presented. The method uses two independent variables for the calculation of the analyte concentration (the amount of sample taken and the amount of analyte added) and one dependent variable, the response. The sensi
A new approach to the nebulization of liquids and its application to atomic absorption spectrophotometry
โ Scribed by R. Bouckaert; J. D'Olieslager; S. De Jaegere
- Publisher
- Elsevier Science
- Year
- 1972
- Tongue
- English
- Weight
- 369 KB
- Volume
- 58
- Category
- Article
- ISSN
- 0003-2670
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โฆ Synopsis
In order to investigate atomization phenomena in premixed flames at low pressure 1, a nebulizer of the total-consumption type had to be built into the low pressure set-up. It is very difficult to run reproducible flame experiments at low pressure with waste liquids accumulating in the vacuum chamber. Therefore a special pneumatic sprayer was developed giving a very high efficiency ( > 9 8 % ) at low pressures. Fortunately this sprayer turned out to have excellent performances, not only at the low pressures for which it was developed (20-100 torr), but also at atmospheric pressure.
This paper reports on the construction of this nebulizer and presents some data on its performance in a normal set-up for atomic absorption measurements at atmospheric pressure. The efficiency of the burner is compared with data from the literature and atomic absorption sensitivities are reported for a few metals.
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