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A New Aldehyde Synthesis—The Reducti[UNK]on of Acid Chlorides by Lithium Tri-t-butoxyaluminohydride 1

✍ Scribed by Brown, Herbert C.; Rao, B. C. Subba

Book ID: 120352648
Publisher: American Chemical Society
Year: 1958
Tongue: English
Weight: 548 KB
Volume: 80
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja01553a014

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3-(4-iodomethyl-2-oxo-1-azetidinyl)propy

3-(4-iodomethyl-2-oxo-1-azetidinyl)propynoic acidt-butyl ester: a new β-lactam derivative, synthesis of an ynamide by reaction of 4-iodomethylazetidin-2-one with the t-butyl ester of propiolic acid in the presence of copper(i)

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The reaction of 4-iodomethylazetidin-2-one ( 2) with the t-butyl ester of propioZic acid (4) in the presence both of equimolar amounts of copper(I) and oxygen results unexpected-Zy in the formation of the $-Zactum ynamide 5. Its structure was suggested by spectroscopic data and confirmed by singLe-c