2-Dimethoxyphosphoryl-1,3-dithiane: A co
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Michael Engelhardt; Gerhard HΓ€gele; Marian Mikolajczyk; Piotr Balczewski; Detlef
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Article
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1985
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John Wiley and Sons
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English
β 403 KB
2-Dimethoxyphosphoryl-l,3-dithiane was obtained by the reaction of 2-ddoro-1,3&thia~~e with trimethyl phosphite. Studies at 200,360 and 400 MHz using 'H, 13C and " P nuclei and lDand 2D NMR techniques are described. Long-range coupling constants were extracted by iterative treatment of [ A B ] , C D