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A Mild and Efficient Method for Chlorination of Baylis–Hillman Adducts Using PPh3/Cl3CCONH2

✍ Scribed by Biswanath Das; Nikhil Chowdhury; Kongara Damodar; Bommena Ravikanth

Publisher
John Wiley and Sons
Year
2007
Tongue
German
Weight
149 KB
Volume
90
Category
Article
ISSN
0018-019X

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✦ Synopsis

Abstract

A new and convenient stereoselective synthesis of (Z)‐2‐(chloromethyl)alk‐2‐enoates has been achieved from Baylis–Hillman adducts by treatment with PPh~3~/Cl~3~CCONH~2~ at room temperature. The synthesis can proceed under mild and acid‐free conditions to form the products in high yields.

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