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A Method for the Optical Resolution of Preparative Scale Quantities of DL-[N-methyl-13C]Carnitine

โœ Scribed by M.C. Madden; M.E. Gokturk; A. Saeed; P.E. Wolkowicz


Book ID
102562367
Publisher
Elsevier Science
Year
1993
Tongue
English
Weight
184 KB
Volume
213
Category
Article
ISSN
0003-2697

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An on-line method for the preparation of
โœ M. Holschbach; M. Schรผller ๐Ÿ“‚ Article ๐Ÿ“… 1993 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 169 KB

An improved on-line synthesis of the powerful methylation reagent, ["CH,]methyl triflate, 1, is described. ## By means of a simple and cheap column technique this reagent is synthesized in an overall reaction time of 12 min in reproducible radiochemical yields of 90% (based on "CO,), a radiochemi