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A method for preparing small quantities of 14C-labeled staphylococcal enterotoxin B

✍ Scribed by John P. Bowden

Book ID
118309061
Publisher
Elsevier Science
Year
1968
Weight
224 KB
Volume
168
Category
Article
ISSN
0005-2795

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πŸ“œ SIMILAR VOLUMES

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## Abstract (l‐^14^C)‐dodecanal was synthesized from (l‐^14^C)‐dodecanoic acid. The two‐step synthesis beginning with 0.9 mg of the acid resulted in an overall yield of 42 % after purification. The final product was separated from the starting material and side products by silicic acid column chrom

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A thod is described for the preparation of 5-bromopentanoic--5 & acid which is inserted the Wittig ylid into the desired prostaglandin intermediate in the 1 ast carbon-carbon bond forming step of the Corey synthesis. Thr diffe nt prostaglandins were prepared carbon-labeled (both pgC and i5Q in the m