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A method for preparing powdered specimens for transmission electron microscopy

โœ Scribed by Carr, Martin J.

Publisher
Wiley (John Wiley & Sons)
Year
1985
Tongue
English
Weight
399 KB
Volume
2
Category
Article
ISSN
0741-0581

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โœฆ Synopsis

A new method of preparing TEM samples from powders is described. The method consists of compacting epoxy-powder composite mixtures in special molds by centrifuging prior to polymerization. The compact is then ion milled by standard methods. Samples prepared in this way are currently being used to study dislocation structures developed during processing of ceramic powders.

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## INTRODUCTION. The high temperature oxidation of alumina-and chromia-forming metals and alloys has been studied for many years. Although it is fairly easy to produce TEM cross-sections of the adherent scales formed on alloys containing reactive elements it has proved more difficult to cross-sect