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A Five-Step Synthesis of Psilocin from Indole-3-carbaldehyde

✍ Scribed by Somei, Masanori; Yamada, Fumio; Tamura, Mayumi

Book ID
111861931
Publisher
Japan Institute of Heterocyclic Chemistry
Year
1998
Tongue
English
Weight
204 KB
Volume
49
Category
Article
ISSN
0385-5414

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A spidamne 2. obtained in two steps from 1.3-butadiene (ca 50 Q). was metho~ycdonylated GHMDS I dimethykarbonate) and akylated wilh idobenzoc+butene (K2CO3 / acetone) to give 8. Heating of I3 kd to the esuane derivative 9 with 6 contnAled centers. The overall yield from I .3-butediene was ca. 32 46.