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A far- and mid-infrared study of HMX (octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine) under high pressure

โœ Scribed by Michael Pravica; Martin Galley; Eunja Kim; Philippe Weck; Zhenxian Liu

Book ID
108109260
Publisher
Elsevier Science
Year
2010
Tongue
English
Weight
951 KB
Volume
500
Category
Article
ISSN
0009-2614

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## Abstract A new series of relatively stable adducts of octahydroโ€1,3,5,7โ€tetranitroโ€1,3,5,7โ€tetrazocine (HMX) with derivatives of pyridineโ€Nโ€oxide were prepared. In addition, relative stable new adducts of HMX were prepared with 5โ€membered, 6โ€membered, and condensedโ€ring heterocyclic compounds. M

Synthesis of 14C-labeled octahydro-1,3,5
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The \({ }^{14} \mathrm{C}\)-uniformly labeled (UL) explosive, octahydro-1,3,5,7-tetranitro-1,3,5,7tetrazocine (HMX) was synthesized in \(40 \%\) yield by nitrolysis of \({ }^{14} \mathrm{C}\)-labeled hexamethylenetetramine (hexamine) in the presence of boron trifluoride diethyl etherate as catalyst.