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A Facile Synthesis of Bis(4-amino-5-mercapto-1,2,4-triazol-3-yl)alkanes and Bis(5-mercapto-4H-1,2,4-triazol-3-yl)alkanes

✍ Scribed by Xu, Peng-Fei; Sun, Xiao-Wen; Zhang, Lin-Mei; Zhang, Zi-Yi


Book ID
115448484
Publisher
Science Reviews 2000 Ltd
Year
1999
Tongue
English
Weight
97 KB
Volume
2
Category
Article
ISSN
0308-2342

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BisΒ­[4-phenyl-5-(1H-1,2,4-triazol-3-yl)-
✍ Pan, Fu-You ;Yang, Jian-Guo ;Chen, Ding-Ben ;Huang, Ling πŸ“‚ Article πŸ“… 2005 πŸ› International Union of Crystallography 🌐 English βš– 235 KB

The title compound, C 20 H 14 N 12 S 2 , was synthesized by the reaction of 3-hydrazino-1H-1,2,4-triazole with phenyl isocyanate in benzene and by ring closure in an alkaline medium. Intermolecular N-HÁ Á ÁN hydrogen bonds are observed and these form a five-membered ring.