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A facile route to a novel aza-crown ether incorporating three thiophene moieties

✍ Scribed by Joan Halfpenny; Phillip B Rooney; Zachary S Sloman

Book ID: 104210655
Publisher: Elsevier Science
Year: 2000
Tongue: French
Weight: 100 KB
Volume: 41
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(00)01033-9

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✦ Synopsis

The preparation of the ®rst of a novel type of large thiophene-containing aza-crown ether is reported. The macrocycle is synthesised by linking a 3,4-dialkoxythiophene moiety with two 3-hydroxythiophene units and ring closure is eected by reaction with piperazine via the Mannich reaction.

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