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A facile micromolar reduction of [1,2,3,4,10-14C]aldrin to 6,7-dihydro[1,2,3,4 10-14C]aldrin

✍ Scribed by Neil J. Lewis; Frederick D. Cazer

Publisher
John Wiley and Sons
Year
1980
Tongue
French
Weight
118 KB
Volume
17
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

The preparation of 6,7‐dihydro[1,2,3,4,10‐^14^C]aldrin is reported by catalytic reduction of [1,2,3,4,10‐^14^C]aldrin. Modification of previously published conditions afforded the desired product in 97.1% yield as assayed by electron capture gas chromatography. The convenient one vessel reaction proceeds rapidly to give the high purity product in twenty minutes at atmospheric pressure.

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