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A di­methyl sulfoxide/chloro­form clathrate of (di­methyl sulfoxide)(tetra­phenyl­porphyrinato)­zinc(II)

✍ Scribed by Vinodu, Mikki ;Goldberg, Israel

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
278 KB
Volume
60
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 110 K Mean '(C±C) = 0.003 A Ê Disorder in solvent or counterion R factor = 0.043 wR factor = 0.112 Data-to-parameter ratio = 14.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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trans-Di-μ-chloro-bis­[(di­methyl sulfoxide-κS)­phenyl­platinum(II)]
✍ Nilsson, Patrik ;Wendt, Ola F. 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 180 KB

The title compound, [Pt 2 Cl 2 (C 6 H 5 ) 2 (C 2 H 6 OS) 2 ] or [Pt("-Cl)Ph(dmso)] 2 (dmso is dimethyl sulfoxide), is a dimer with a pseudo square-planar coordination geometry around the Pt atoms, with two bridging Cl ligands creating a four-membered ring at the centre of the dimer. The complex is c