A crystal structure determination of titanium(II) tetrachloroaluminate by vibrational correlation methods and powder diffraction
β Scribed by A. Justnes; E. Rytter; A.F. Andresen
- Book ID
- 108428192
- Publisher
- Elsevier Science
- Year
- 1982
- Tongue
- English
- Weight
- 337 KB
- Volume
- 1
- Category
- Article
- ISSN
- 0277-5387
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Two new compounds, Rb 2 (HSO 4 )(H 2 PO 4 ) and Rb 4 (HSO 4 ) 3 (H 2 PO 4 ), were synthesized from aqueous solutions of RbHSO 4 /RbH 2 PO 4 . The compounds were characterized by Xray single crystal analysis and neutron powder di4raction. For Rb 2 (HSO 4 )(H 2 PO 4 ), room temperature and a low tempe
## Synchrotron powder data on as-synthesized AlPOd-was indexed on a cubic cell with a = 13.3832(6) A and systematic absences of hkl with h + k, h + I, k + I = odd and hhl with h + I = odd. The most probable space group is f23 (#196), assuming alternation of the aluminum and phosphorus atoms. The f