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A Convenient Synthesis of Unsymmetrical N,N′-Disubstitutedα,ω-Diaminoalkanes

✍ Scribed by Orelli, Liliana R.; Salerno, Alejandra; Hedrera, Mónica E.; Perillo, Isabel A.

Book ID
115517743
Publisher
Taylor and Francis Group
Year
1998
Tongue
English
Weight
443 KB
Volume
28
Category
Article
ISSN
0039-7911

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📜 SIMILAR VOLUMES

ChemInform Abstract: A Convenient Synthe
ChemInform Abstract: A Convenient Synthesis of Unsymmetrical N,N′-Disubstituted α,ω-Diaminoalkanes.
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An efficient and practical method for th
An efficient and practical method for the synthesis of mono-N-protected α,ω-diaminoalkanes
✍ Jae Wook Lee; Sung Im Jun; Kimoon Kim 📂 Article 📅 2001 🏛 Elsevier Science 🌐 French ⚖ 61 KB

The large-scale synthesis of mono-N-protected (Cbz, Boc, Ts, and Ns) a,v-diaminoalkanes (the number of carbon atoms=3, 4, 5 and 6) are accomplished in 81-94% yield by the protection of amine and subsequent reduction of an azido group from a,v-azido alkyl amines. a,v-Azido alkyl amines are prepared e