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A convenient synthesis of secondary hydroxylamines

✍ Scribed by Ian A O'Neil; Ed Cleator; David J Tapolczay

Publisher
Elsevier Science
Year
2001
Tongue
French
Weight
95 KB
Volume
42
Category
Article
ISSN
0040-4039

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✦ Synopsis

The oxidation of a range of b-cyanoethyl tertiary amines with mCPBA gives the corresponding N-oxides, which can be isolated or undergo Cope-elimination to give secondary hydroxylamines in excellent yield.

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