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A CONVENIENT SYNTHESIS OF 2,3-DICHLORO-1,4-NAPHTHOQUINONE-1-14C USING A NOVEL CHLORINATION PROCEDURE

✍ Scribed by Ehler, Kenneth W.; Pardini, Ronald S.

Book ID
115528261
Publisher
Taylor and Francis Group
Year
1983
Tongue
English
Weight
200 KB
Volume
15
Category
Article
ISSN
0030-4948

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The pyrrolo [2,l-c][1,4]benzoxazine system was synthesized from 2-fluoroaniline involving an intramolecular nucleophilic displacement of the fluoride atom. The intermediate alcohols 7a and 10 were treated in basic media under strictly controlled conditions which led to the desired tricyclic structur