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A Convenient Procedure for the Synthesis of 6- O -Mono-Phosphate β-Cyclodextrins

✍ Scribed by Simelane, Siphamandla; Mamba, Brillance Bhekie; Mbianda, Xavier Yangkou

Book ID
121278689
Publisher
Taylor and Francis Group
Year
2013
Tongue
English
Weight
195 KB
Volume
188
Category
Article
ISSN
1042-6507

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Mono-6-(O-2,4,6-triisopropylbenzenesulfo
Mono-6-(O-2,4,6-triisopropylbenzenesulfonyl)-γ-cyclodextrin, a novel intermediate for the synthesis of mono-functionalised γ-cyclodextrins
✍ Ronald Palin; Simon J.A Grove; Alan B Prosser; Ming-Qiang Zhang 📂 Article 📅 2001 🏛 Elsevier Science 🌐 French ⚖ 131 KB

A reaction between g-cyclodextrin (g-CD) and 2,4,6-triisopropylbenzenesulfonyl chloride in pyridine gave mono-6-(O-2,4,6-triisopropylbenzenesulfonyl)-g-cyclodextrin in good yield ( 69%) and high purity (>98%). In contrast to other sulfonylations of g-CD, this reaction did not give di-or tri-substitu