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A cold silanization method for preparation of medium polarity capillary columns

✍ Scribed by Traitler, H.

Publisher
John Wiley and Sons
Year
1983
Tongue
English
Weight
290 KB
Volume
6
Category
Article
ISSN
0935-6304

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✦ Synopsis

Abstract

Silane‐coupling agents, commonly used for fiberglass reinforced plastics (FRP), were applied for deactivation of silanol sites in glass capillary columns prior to coating with mediumpolarity phases such as Carbowax and Superox. The columns, prepared in a two‐stage process in the case of glass (acidic leaching and drying, dynamic cold silanization followed by static coating with the phase) or a one stage process in the case of fused silica, gave the best results when deactivation and hence wettability were induced by glycidoxypropyltrimethoxy silane.

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