A cocrystal of 3-nitrophenylanilinium perchlorate and 3-nitroaniline
✍ Scribed by Bao, Feng ;Chen, Ying ;Ng, Seik Weng
- Book ID
- 104487700
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 141 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
No coin nor oath required. For personal study only.
✦ Synopsis
all atoms except one O atom of the perchlorate ion and two H atoms bonded to nitrogen lie on a mirror plane. Hydrogen bonds link the cation, anion and neutral molecule into a chain that runs along the c axis of the orthorhombic unit cell.
📜 SIMILAR VOLUMES
## Abstract Five steps were required to synthesize the title compound. This involved a catalytic exchange reaction, nitration, hydrolysis, and condensation. The overall radiochemical yield was 28.87% and the specific activity was 12.4 mCi/mmol, with a radiochemical purity of more than 95.7%.
I3C chemical shifts are reported for a series of nitro and phenyl derivatives of 2-and 3-methylindoles and 2-and 3-formylindoles, measured in DMSO-d,. The I3C substituent chemical shift (SCS) data are discussed and compared with ' H SCS data.