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A 13C NMR study of the Mn2+ · bleomycin complex

✍ Scribed by Robert P. Sheridan; Raj K. Gupta

Book ID
115912364
Publisher
Elsevier Science
Year
1981
Tongue
English
Weight
410 KB
Volume
134
Category
Article
ISSN
0014-5793

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Complete assignment of the 13C NMR spect
Complete assignment of the 13C NMR spectra of bleomycin A2 and its zinc complex by means of two-dimensional NMR spectroscopy
✍ M. A. J. Akkerman; C. A. G. Haasnoot; U. K. Pandit; C. W. Hilbers 📂 Article 📅 1988 🏛 John Wiley and Sons 🌐 English ⚖ 757 KB

13C NMR spectra of free bleomycin A, at pH 4 and 6.7 and of its zinc complex at pH 6.7 were completely assigned by making use of two-dimensional 'H-"C correlated spectroscopy. Differences in resonance positions between the spectra of the free bleomycin at pH 4 and 6.7 are observed for the /?-hydroxy