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Location of iron in the Fe2+-bleomycin complex as observed by 13C NMR spectroscopy

✍ Scribed by Raj K. Gupta; James A. Ferretti; William J. Caspary

Book ID
118313374
Publisher
Elsevier Science
Year
1979
Tongue
English
Weight
476 KB
Volume
89
Category
Article
ISSN
0006-291X

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Complete assignment of the 13C NMR spect
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13C NMR spectra of free bleomycin A, at pH 4 and 6.7 and of its zinc complex at pH 6.7 were completely assigned by making use of two-dimensional 'H-"C correlated spectroscopy. Differences in resonance positions between the spectra of the free bleomycin at pH 4 and 6.7 are observed for the /?-hydroxy