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A 13 C CP/MAS NMR Study of the Structure and Dynamics of [(η 5 -C 5 H 5 ) 2 Fe 2 (CO) 4 ] Included in γ-Cyclodextrin: Evidence for Terminal−Bridging Exchange in the cis Isomer

✍ Scribed by Canuto, Holly C.; Masic, Admir; Rees, Nicholas H.; Heyes, Stephen J.; Gobetto, Roberto; Aime, Silvio


Book ID
124056341
Publisher
American Chemical Society
Year
2006
Tongue
English
Weight
97 KB
Volume
25
Category
Article
ISSN
0276-7333

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13C CP-MAS NMR spectra and fluxional beh
✍ M. V. Galakhov; V. I. Bakhmutov; I. V. Barinov 📂 Article 📅 1991 🏛 John Wiley and Sons 🌐 English ⚖ 180 KB

## Abstract Internal rotation about the C‐2–C‐3 bond was observed in the ^13^C CP‐MAS NMR spectra of the solid complexes [M~2~(ηHC^1^C^2^C^3^Me~2~)(CO)~4~(ηC~5~H~5~)~2~]^+^ [BF~4~]^−^ where M = Mo or W.